New developments in high-pressure X-ray diffraction beamline for diamond anvil cell at SPring-8

Hirao N.; Kawaguchi S. I.; Hirose K.; Shimizu K.; Ohtani E.; Ohishi Y.

doi:10.1063/1.5126038

Volume 5 Issue 1

Jan. 2020

Turn off MathJax

Article Contents

Article Navigation > Matter and Radiation at Extremes > 2020 > 5(1): 018403

Hirao N., Kawaguchi S. I., Hirose K., Shimizu K., Ohtani E., Ohishi Y.. New developments in high-pressure X-ray diffraction beamline for diamond anvil cell at SPring-8[J]. Matter and Radiation at Extremes, 2020, 5(1): 018403. doi: 10.1063/1.5126038

Citation:

Hirao N., Kawaguchi S. I., Hirose K., Shimizu K., Ohtani E., Ohishi Y.. New developments in high-pressure X-ray diffraction beamline for diamond anvil cell at SPring-8[J]. Matter and Radiation at Extremes, 2020, 5(1): 018403. doi: 10.1063/1.5126038

Citation:

PDF( 5543 KB)

New developments in high-pressure X-ray diffraction beamline for diamond anvil cell at SPring-8

doi: 10.1063/1.5126038

Hirao N.^{1
,
,
,},
Kawaguchi S. I.¹,
Hirose K.^{2, 3},
Shimizu K.⁴,
Ohtani E.⁵,
Ohishi Y.¹

1.
Japan Synchrotron Radiation Research Institute, Sayo, Hyogo 679-5198, Japan
2.
Department of Earth and Planetary Science, The University of Tokyo, Tokyo 113-0033, Japan
3.
Earth-Life Science Institute, Tokyo Institute of Technology, Tokyo 152-8550, Japan
4.
Center of Science and Technology Under Extremes Conditions, Graduate School of Engineering Science, Osaka University, Osaka 560-8531, Japan
5.
Department of Earth Science, Graduate School of Science, Tohoku University, Sendai 980-8578, Japan

More Information

Corresponding author: a)Author to whom correspondence should be addressed: hirao@spring8.or.jp
Received Date: 2019-08-28
Accepted Date: 2019-12-08

Available Online: 2020-01-15

Publish Date: 2020-01-15

Abstract

Abstract

An overview of the recently renovated high-pressure X-ray diffraction (XRD) BL10XU beamline for the diamond anvil cell at SPring-8 is presented. The renovation includes the replacement of the X-ray source and monochromator, enhanced focusing systems for high-energy XRD, and recent progress in the sample environment control techniques that are available for high-pressure studies. Other simultaneous measurement techniques for combination with XRD, such as Raman scattering spectroscopy and Mössbauer spectroscopy, have been developed to obtain complementary information under extreme conditions. These advanced techniques are expected to make significant contributions to in-depth understanding of various and complicated high-pressure phenomena. The experience gained with the BL10XU beamline could help promote high-pressure research in future synchrotron radiation facilities.

FullText(HTML)

References(43)

References

[1]	M. Mezouar, W. A. Crichton, S. Bauchau, F. Thurel, H. Witsch, F. Torrecillas, G. Blattmann, P. Marion, Y. Dabin, J. Chavanne, O. Hignette, C. Morawe, and C. Borel, “Development of a new state-of-the-art beamline optimized for monochromatic single-crystal and powder X-ray diffraction under extreme conditions at the ESRF,” J. Synchrotron Radiat. 12, 659 (2005).10.1107/s0909049505023216 doi: 10.1107/s0909049505023216
[2]	G. Shen, V. B. Prakapenka, P. J. Eng, M. L. Rivers, and S. R. Sutton, “Facilities for high-pressure research with the diamond anvil cell at GSECARS,” J. Synchrotron Radiat. 12, 642 (2005).10.1107/s0909049505022442 doi: 10.1107/s0909049505022442
[3]	Y. Meng, R. Hrubiak, E. Rod, R. Boehler, and G. Shen, “New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team,” Rev. Sci. Instrum. 86, 072201 (2015).10.1063/1.4926895 doi: 10.1063/1.4926895
[4]	Y. Ohishi, N. Hirao, N. Sata, K. Hirose, and M. Takata, “Highly intense monochromatic X-ray diffraction facility for high-pressure research at SPring-8,” High Pressure Res. 28, 163 (2008).10.1080/08957950802208910 doi: 10.1080/08957950802208910
[5]	H.-P. Liermann, Z. Konôpková, W. Morgenroth, K. Glazyrin, J. Bednarčik, E. E. McBride, S. Petitgirard, J. T. Delitz, M. Wendt, Y. Bican, A. Ehnes, I. Schwark, A. Rothkirch, M. Tischer, J. Heuer, H. Schulte-Schrepping, T. Kracht, and H. Franz, “The extreme conditions beamline P02.2 and the extreme conditions science infrastructure at PETRA III,” J. Synchrotron Radiat. 22, 908 (2015).10.1107/s1600577515005937 doi: 10.1107/s1600577515005937
[6]	M. Murakami, K. Hirose, K. Kawamura, N. Sata, and Y. Ohishi, “Post-perovskite phase transition in MgSiO3,” Science 304, 855 (2004).10.1126/science.1095932 doi: 10.1126/science.1095932
[7]	H. Fujihisa, Y. Akahama, H. Kawamura, Y. Ohishi, O. Simomura, H. Yamawaki, M. Sakashita, Y. Gotoh, S. Takeya, and K. Honda, “O8 cluster structure of the epsilon phase of solid oxygen,” Phys. Rev. Lett. 97, 085503 (2006).10.1103/physrevlett.97.085503 doi: 10.1103/physrevlett.97.085503
[8]	S. Tateno, K. Hirose, Y. Ohishi, and Y. Tatsumi, “The structure of iron in Earth’s inner core,” Science 330, 359 (2010).10.1126/science.1194662 doi: 10.1126/science.1194662
[9]	R. Kinjo, A. Kagamihata, T. Seike, H. Kishimoto, H. Ohashi, S. Yamamoto, and T. Tanaka, “Lightweight-compact variable-gap undulator with force cancellation system based on multipole monolithic magnets,” Rev. Sci. Instrum. 88, 073302 (2017).10.1063/1.4991652 doi: 10.1063/1.4991652
[10]	M. Yabashi, K. Tono, H. Mimura, S. Matsuyama, K. Yamauchi, T. Tanaka, H. Tanaka, K. Tamasaku, H. Ohashi, S. Goto, and T. Ishikawa, “Optics for coherent X-ray applications,” J. Synchrotron Radiat. 21, 976 (2014).10.1107/s1600577514016415 doi: 10.1107/s1600577514016415
[11]	M. Yabashi, H. Yamazaki, K. Tamasaku, S. Goto, S. K. Takeshita, T. Mochizuki, Y. Yoneda, Y. Furukawa, and T. Ishikawa, “SPring-8 standard x-ray monochromators,” Proc. SPIE 3773, 2 (1999).10.1117/12.370098 doi: 10.1117/12.370098
[12]	T. Mochizuki, Y. Kohmura, A. Awaji, Y. Suzuki, A. Barona, K. Tamasaku, M. Yabashi, H. Yamazaki, and T. Ishikawa, “Cryogenic cooling monochromators for the SPring-8 undualtor beamlines,” Nucl. Instrum. Methods Phys. Res. A 467-468, 647 (2001).10.1016/s0168-9002(01)00436-3 doi: 10.1016/s0168-9002(01)00436-3
[13]	H. Yamazaki, H. Ohashi, Y. Senba, T. Takeuchi, Y. Shimizu, M. Tanaka, Y. Matsuzaki, H. Kishimoto, T. Miura, Y. Terada, M. Suzuki, H. Tajiri, S. Goto, M. Yamamoto, M. Takata, and T. Ishikawa, “Improvement in stability of SPring-8 X-ray monochromators with cryogenic-cooled silicon crystals,” J. Phys. Conf. Ser. 425, 052001 (2013).10.1088/1742-6596/425/5/052001 doi: 10.1088/1742-6596/425/5/052001
[14]	Y. Ohishi, A. Q. R. Baron, M. Ishii, T. Ishikawa, and O. Shimomura, “Refractive x-ray lens for high pressure experiments at SPring-8,” Nucl. Instrum. Methods Phys. Res. A 467-468, 962 (2001).10.1016/s0168-9002(01)00541-1 doi: 10.1016/s0168-9002(01)00541-1
[15]	V. Nazmov, E. Reznikova, A. Somogyi, J. Mohr, and V. Saile, “Planar sets of cross X-ray refractive lenses from SU-8 polymer,” Proc. SPIE 5539, 235–243 (2004).10.1117/12.562615 doi: 10.1117/12.562615
[16]	Y. Akahama, N. Hirao, Y. Ohishi, and A. K. Singh, “Equation of state of bcc-Mo by static volume compression to 410 GPa,” J. Appl. Phys. 116, 223504 (2014).10.1063/1.4903940 doi: 10.1063/1.4903940
[17]	T. Sakai, T. Yagi, H. Ohfuji, T. Irifune, Y. Ohishi, N. Hirao, Y. Suzuki, Y. Kuroda, T. Asakawa, and T. Kanemura, “High-pressure generation using double stage micro-paired diamond anvils shaped by focused ion beam,” Rev. Sci. Instrum. 86, 033905 (2015).10.1063/1.4914844 doi: 10.1063/1.4914844
[18]	T. Sakai, T. Yagi, T. Irifune, H. Kadobayashi, N. Hirao, T. Kunimoto, H. Ohfuji, S. Kawaguchi-Imada, Y. Ohishi, S. Tateno, and K. Hirose, “High pressure generation using double-stage diamond anvil technique: Problems and equations of state of rhenium,” High Pressure Res. 38, 107 (2018).10.1080/08957959.2018.1448082 doi: 10.1080/08957959.2018.1448082
[19]	S. Desgreniers, J. S. Tse, T. Matsuoka, Y. Ohishi, Q. Li, and Y. Ma, “High pressure–low temperature phase diagram of barium: Simplicity versus complexity,” Appl. Phys. Lett. 107, 221908 (2015).10.1063/1.4936849 doi: 10.1063/1.4936849
[20]	Y. Takabayashi, A. Y. Ganin, P. Jeglič, D. Arčon, T. Takano, Y. Iwasa, Y. Ohishi, M. Takata, N. Takeshita, K. Prassides, and M. J. Rosseinsky, “The disorder-free non-BCS superconductor Cs3C60 emerges from an antiferromagnetic insulator parent state,” Science 323, 1585 (2009).10.1126/science.1169163 doi: 10.1126/science.1169163
[21]	T. Watanuki, O. Shimomura, T. Yagi, T. Kondo, and M. Isshiki, “Construction of laser-heated diamond anvil cell system for in situ x-ray diffraction study at SPring-8,” Rev. Sci. Instrum. 72, 1289 (2001).10.1063/1.1343869 doi: 10.1063/1.1343869
[22]	K. Ohta, S. Onoda, K. Hirose, R. Sinmyo, K. Shimizu, N. Sata, Y. Ohishi, and A. Yasuhara, “The electrical conductivity of post-perovskite in Earth’s D” layer,” Science 320, 89 (2008).10.1126/science.1155148 doi: 10.1126/science.1155148
[23]	K. Ohta, Y. Kuwayama, K. Hirose, K. Shimizu, and Y. Ohishi, “Experimental determination of the electrical resistivity of iron at Earth’s core conditions,” Nature 534, 95 (2016).10.1038/nature17957 doi: 10.1038/nature17957
[24]	J. Binns, P. Dalladay-Simpson, M. Wang, G. J. Ackland, E. Gregoryanz, and R. Howie, “Formation of H2-rich iodine-hydrogen compounds at high pressure,” Phys. Rev. B 97, 024111 (2018).10.1103/physrevb.97.024111 doi: 10.1103/physrevb.97.024111
[25]	M. Murakami, Y. Asahara, Y. Ohishi, N. Hirao, and K. Hirose, “Development of in situ Brillouin spectroscopy at high pressure and high temperature with synchrotron radiation and infrared laser heating system: Application to the Earth’s deep interior,” Phys. Earth Planet. Inter. 174, 282 (2009).10.1016/j.pepi.2008.07.030 doi: 10.1016/j.pepi.2008.07.030
[26]	M. Murakami, Y. Ohishi, N. Hirao, and K. Hirose, “A perovskitic lower mantle inferred from high-pressure, high-temperature sound velocity data,” Nature 485, 90 (2012).10.1038/nature11004 doi: 10.1038/nature11004
[27]	Y. Kudo, K. Hirose, M. Murakami, Y. Asahara, H. Ozawa, Y. Ohishi, and N. Hirao, “Sound velocity measurements of CaSiO3 perovskite to 133 GPa and implications for lowermost mantle seismic anomalies,” Earth Planet. Sci. Lett. 349-350, 1 (2012).10.1016/j.epsl.2012.06.040 doi: 10.1016/j.epsl.2012.06.040
[28]	Y. Asahara, K. Hirose, Y. Ohishi, N. Hirao, H. Ozawa, and M. Murakami, “Acoustic velocity measurements for stishovite across the post-stishovite phase transition under deviatoric stress: Implications for the seismic features of subducting slabs in the mid-mantle,” Am. Mineral. 98, 2053 (2013).10.2138/am.2013.4145 doi: 10.2138/am.2013.4145
[29]	Y. Akahama and H. Kawamura, “High-pressure Raman spectroscopy of diamond anvils to 250 GPa: Method for pressure determination in the multimegabar pressure range,” J. Appl. Phys. 96, 3748 (2004).10.1063/1.1778482 doi: 10.1063/1.1778482
[30]	Y. Akahama and H. Kawamura, “Pressure calibration of diamond anvil Raman gauge to 310 GPa,” J. Appl. Phys. 100, 043516 (2006).10.1063/1.2335683 doi: 10.1063/1.2335683
[31]	Y. Akahama, M. Nishimura, H. Kawamura, N. Hirao, Y. Ohishi, and K. Takemura, “Evidence from x-ray diffraction of orientational ordering in phase III of solid hydrogen at pressures up to 183 GPa,” Phys. Rev. B 82, 060101(R) (2010).10.1103/physrevb.82.060101 doi: 10.1103/physrevb.82.060101
[32]	Y. Akahama, T. Maekawa, T. Sugimoto, H. Fujihisa, N. Hirao, and Y. Ohishi, “High-pressure phase diagram of O2 and N2 binary system: formation of kagome-lattice of O2,” J. Phys. Conf. Ser. 500, 182001 (2014).10.1088/1742-6596/500/18/182001 doi: 10.1088/1742-6596/500/18/182001
[33]	Y. Akahama, D. Ishihara, H. Yamashita, H. Fujihisa, N. Hirao, and Y. Ohishi, “Phase stability and magnetic behavior of hexagonal phase of N2–O2 system with Kagome lattice under high pressure and low temperature,” Phys. Rev. B 94, 064104 (2016).10.1103/physrevb.94.064104 doi: 10.1103/physrevb.94.064104
[34]	M. Einaga, M. Sakata, T. Ishikawa, K. Shimizu, M. I. Eremets, A. P. Drozdov, I. A. Troyan, N. Hirao, and Y. Ohishi, “Crystal structure of the superconducting phase of sulfur hydride,” Nat. Phys. 12, 835 (2016).10.1038/nphys3760 doi: 10.1038/nphys3760
[35]	T. Matsuoka and K. Shimizu, “Direct observation of a pressure-induced metal-to-semiconductor transition in lithium,” Nature 458, 186 (2009).10.1038/nature07827 doi: 10.1038/nature07827
[36]	T. Matsuoka, M. Sakata, Y. Nakamoto, K. Takahama, K. Ichimaru, K. Mukai, K. Ohta, N. Hirao, Y. Ohishi, and K. Shimizu, “Pressure-induced reentrant metallic phase in lithium,” Phys. Rev. B 89, 144103 (2014).10.1103/physrevb.89.144103 doi: 10.1103/physrevb.89.144103
[37]	M. Sakata, Y. Nakamoto, K. Shimizu, T. Matsuoka, and Y. Ohishi, “Superconducting state of Ca-VII below a critical temperature of 29 K at a pressure of 216 GPa,” Phys. Rev. B 83, 220512(R) (2011).10.1103/physrevb.83.220512 doi: 10.1103/physrevb.83.220512
[38]	T. Mitsui, N. Hirao, Y. Ohishi, R. Masuda, Y. Nakamura, H. Enoki, K. Sakaki, and M. Seto, “Development of an energy-domain 57Fe-Mössbauer spectrometer using synchrotron radiation and its application to ultrahigh-pressure studies with a diamond anvil cell,” J. Synchrotron Radiat. 16, 723 (2009).10.1107/s0909049509033615 doi: 10.1107/s0909049509033615
[39]	V. Potapkin, A. I. Chumakov, G. V. Smirnov, J.-P. Celse, R. Rüffer, C. McCammon, and L. Dubrovinsky, “The 57Fe synchrotron Mössbauer source at the ESRF,” J. Synchrotron Radiat. 19, 559 (2012).10.1107/s0909049512015579 doi: 10.1107/s0909049512015579
[40]	S. Kamada, N. Suzuki, F. Maeda, N. Hirao, M. Hamada, E. Ohtani, R. Masuda, T. Mitsui, Y. Ohishi, and S. Nakano, “Electronic properties and compressional behavior of Fe–Si alloys at high pressure,” Am. Mineral. 103, 1959 (2018).10.2138/am-2018-6425 doi: 10.2138/am-2018-6425
[41]	F. Maeda, S. Kamada, E. Ohtani, N. Hirao, T. Mitsui, R. Masuda, M. Miyahara, and C. McCammon, “Spin state and electronic environment of iron in basaltic glass in the lower mantle,” Am. Mineral. 102, 2106 (2017).10.2138/am-2017-6035 doi: 10.2138/am-2017-6035
[42]	T. Tanaka and H. Kitamura, “SPECTRA: A synchrotron radiation calculation code,” J. Synchrotron Radiat. 8, 1221 (2001).10.1107/s090904950101425x doi: 10.1107/s090904950101425x
[43]	This work was performed at the SPring-8 facility with the approval of the Japan Synchrotron Radiation Research Institute (Proposals Nos. 2009A2021, 2009B2131, 2010A1232, 2010A1966, 2014A1910, 2014A1911, 2014B2059, 2015A2066, 2015B2001, 2016A1846, 2016A1853, 2016A1854, 2016B1960, 2017A1870, 2017B1986, 2017B1987, and 2018A2073).